Which one of the following mixtures can be separated by steam distillation technique?

Glycerol is purified by

The correct match between items of List-$I$ and List-$II$ is:

List-$I$	List-$II$
$A$. Coloured impurity	$P$. Steam distillation
$B$. Mixture of $o$-nitrophenol and $p$-nitrophenol	$Q$. Fractional distillation
$C$. Crude oil	$R$. Charcoal treatment
$D$. Mixture of glycerol and sugars	$S$. Distillation under reduced pressure

Fill in the blanks:
$1$. In differential extraction from two layers,the .......... layer is above because .............
$2$. The organic solvent used in differential extraction is .......... in water.
$3$. If an organic compound is ......... soluble in an organic solvent,then the continuous extraction technique is used.
$4$. ........ solution is added to produce the precipitate of halide for the estimation of halogen.

On a thin layer chromatographic plate,an organic compound moved by $3.5 \ cm$,while the solvent moved by $5 \ cm$. The retardation factor of the organic compound is . . . . . . $\times 10^{-1}$.

Using the given figure,the ratio of $R_f$ values of sample $A$ and sample $C$ is $x \times 10^{-2}$. The value of $x$ is . . . . . . . .
Table: Paper chromatography of Samples
| Component | Distance from base line (cm) |
| :--- | :--- |
| Sample $A$ | $5.0$ |
| Sample $B$ | $6.5$ |
| Sample $C$ | $10.0$ |
| Solvent front | $12.5$ |